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SS2100 - High Range H2O GTL/SynGas (Sasol Process)

Tunable Diode Laser technology is perfect for fast, sensitive H2O measurements in Synthol Reactor Tail Gas Scrubber applications. Synthol Process The Synthol process starts with synthesis gas from coal or natural gas to make hydrocarbon liquids and waxes in a Fischer-Tropsch reactor. The liquids are separated and refined to make transportation fuels and chemicals.
Product Code: 65601
 
 
 
 
 

Application Note

Critical Control of Moisture
Moisture must be removed prior to downstream cryogenic recovery and separation of the C2 and C3 hydrocarbons present. Fixed bed desiccant dryers are often used to remove the moisture (Fig. 1). Two beds are normal, with one in service while the other is being regenerated. Sometimes, two beds are used in series with a moisture monitor between the sample beds. When the first bed is exhausted it is regenerated and becomes the second bed after regeneration.

Traditional Measurement Solutions
Aluminum Oxide capacitance probes, electrochemical and vibrating quartz crystal moisture analyzers have been the traditional method for monitoring the levels of H2O in Desiccant Dryer Outlets. Unfortunately, trace hydrocarbons and other contaminants present in the stream contaminate the capacitance and electrochemical probes, resulting in high maintenance costs due to the need to be constantly replaced. It’s not uncommon for moisture probes to be replaced multiple times a year. Quartz crystal moisture meters have slow wet-up and dry-down times that are slow to detect break-through from the dryers.

SpectraSensors’ Solution
SpectraSensors SS2100 is the ideal solution for wet gas applications. Its non-contact laser and detector are impervious to damage from contaminants. Tunable Diode Laser technology means that measurement interferences from other infrared absorbing compounds are avoided. There are no wet-up or dry-down delays, resulting in fast updates even when the concentration changes dramatically (Fig. 2).

High water concentrations (>50 ppm) are easily measured without Differential Spectroscopy, so there are no consumable parts or utilities other than electrical power. The SS2100 has no routine maintenance requirement and laser diodes last for many years so the cost of ownership is very low.


Typical Stream Composition

Component

Unit

Typical Concentration

Min. for Application

Max. for Application

H2O

ppmv

500

20

1000

Carbon Dioxide (CO2)

ppmv

100

2

1000

Hydrogen (H2)

Mole%

43.5

35

 

55

 

Nitrogen (N2)

Mole%

0.55

0.2

1

Carbon Monoxide (CO)

Mole%

2.85

2.2

3.4

Argon (Ar)

Mole%

3.4

4.29

5.2

C2’s

Mole%

38.3

31

47

C3’s

Mole%

2.2

0.4

3.4

C4’s

Mole%

0.3

0.2

2

C5’s

Mole%

0.1

0.02

0.2

C6’s

Mole%

0.02

0.01

0.1

Total

Mole%

100

 

 

 

The background stream composition must be specified for proper calibration and measurement performance. Specify the Normal composition, along with the minimum and maximum expected values for each component, especially water, the measured component. Other stream compositions may be allowable with approval from SpectraSensors. 

 
 
 
 

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Data Sheet


Performance

Target Components

H2O in GTL/SynGas (Sasol Process)

Typical Measurement Ranges

20 - 100 ppm  through 0-1000ppm
(specify range)*

Typical Precision

 ±2% of Full Scale*

Measurement Response Time

1 to ~60 sec*

Principle of Measurement

Tunable Diode Laser Absorption Spectroscopy
Non-differential

Environmental Temperature Range

-20º to 50ºC (-4º to 122ºF)
-10º to 60ºC (14º to 140ºF) optional

Sample Inlet Pressure

70 kPag (10 psig) typical

210 kPag (30 psig) maximum


Cell Temperature

Maintain at 50ºC +/- 0.2ºC

Maximum Cell Pressure

70 kPag (10 PSIg)

Sample Flow Rate
 
1 - 2 L/min (2.1 to 4.2 scfh)*
Validation
Certified blend of H2O in Nitrogen balance
 

Electrical

Power

100-240 VAC, 50-60 Hz standard

Max Current

Controller: 1 A @ 120 VAC

Controller to Cell Cable Length

1m standard (3m, 5m & 10m available optionally)

Communication

Current Loop Output 4-20 mA Isolated,
1200 ohms @ 24 VDC max load
Serial: ASCII Text RS232C standard
Modbus RS232C
Digital Outputs
4 ea. 12 VDC for valve operations
Scrubber (if required), Process/Val, Val 1, Val 2
5 SPDT (Form C) Dry Contact Alarms
Common Fault, Val 1 Active, Val 2 Active, Val Fail,
one user-assignable to any alarm 
LCD Display
Concentration, Cell Pressure and Temperature, Diagnostic Data
 

Physical

Controller Enclosure

NEMA 4X - 304 Stainless Steel standard

Controller Dimensions

343mm H x 305mm W x 165mm H
(13.5" H x 12" W x 6-7/16" D)*

Weight Approximately

13.1 Kg (28.6 lbs)*

Sample Cell Dimensions

0.8m cell
438 mm H × 108 mm W
(17-1/4” H × 4-1/4” W)*

Sample Cell Construction

316L Series Polished Stainless Steel standard
Number of Sample Cells
1 (single channel SS2100) or
2 (dual channel SS2100)
Area Classification
CSA Certified for Class I, Division 2,
Groups ABCD Temp Code T3C
 ll 2G Ex d llB+H2 T5; Tamb : -20 ÷ +60 °C
Dimensions with Sample System 1678 mm H x 613 mm W x 427 mm D
(66” H x 24-1/8” W x 16-13/16” D)
Weight with Sample System (approx.) 68 kg (150 lbs.)

* Application specific; consult factory

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Drawings

 
 

Typical Accessories


SS2100 ARM9 Electronics
 

80000-02199

Temperature Control Board

23000-00030

4-20 mA Current Loop Board
 

80000-02203

Power Supply Assembly, 120/240 VAC 50/60 Hz
 

80000-02300

Power Supply Assembly, 24 VDC
 

01902-17106 External Serial Output Cable

01902-30011 Keypad Assembly

24601-00002
Display Assembly
 
02203-13100
Daughter Board
 
45000-02002
Relay, DC12V SPDT 3 A/120 VAC
 

Cell (0.8m)
01902-17102
Pressure Transducer Assembly
 
02199-00001
Spares/Cleaning Kit (o-rings, fuses), AC, Viton (domestic only)
 
02199-00005
Spares Kit (o-rings, fuses), AC, Viton
 
 
 

Photos

 
 

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